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Wednesday, February 27, 2013

Experiment 11

Discussion & Conclusion
In this try out we learned how to compound the cyclohexene by dehydration of cyclohexanol. We procedure the first step where we film to mix the components. Then we heat the R.B.F with a fractionating column, distilled water. Then we obtained the layers, and we transferred the organic fertiliser layer to a small, dry Erlenmeyer flask. We added anhydrous Sodium convert as a drying agent. To complete, we distilled the cyclohexene and collected the intersection. Knowing this data, we determined the give up % which is 58.5%. This experiment features the dehydration of cyclohexanol and produce cyclohexene. The acid catalyzed dehydration of cyclohexanol with distillative removal of the resulting cyclohexene from the reaction mixture is a very good pillow slip to show the possibility of combining two steps in synthesis in one single step, reducing the experiment time length, and the possibilities of side reactions. This technique of distillation of the product as it forms, is only applicable to a small group of reactions where the product of reaction have the lowest boiling point among the reactants. This technique prevents the product to contact other reactants, and leave the heating purlieu which might cause side reactions.

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The removal of the product in like manner helps to shift the equilibrium position of the incomplete reaction to the proficient hand side, and prevents backwards reaction, resulting in an increased yield of products. A side reaction is an unwanted chemical reaction fetching place that diminishes the yield of the desired product. The amount of product in a chemical synthesis is the reaction yield. Typically, chemical yields be expressed as a weight in grams or as a percentage of the total theoretical quantity of product that could be produced. Due to the presence of the hot pure sulphuric acid, the product cyclohexene may also be subjected to raise oxidation. The double bond may be oxidized to a di-aldehyde or other fragments. This synthesis...If you want to get a climb essay, order it on our website: Orderessay



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